HPLC

Analysis of Dicamba and 2,4-D by Shimadzu’s Triple Quad LCMS-8060

Shimadzu’s app note demonstrates the sensitivity of the LCMS-8060 when analyzing dicamba and 2,4-D in a solution of 100x diluted glufosinate herbicide that contains a high amount of surfactants and other potential mass spec interferants.

The LC/MS/MS method was quickly developed with readily available mobile phases. Dicamba in methanol 0.01 and 0.025 ppb had a S/N of 3/1 and 10/1, respectively. 2,4-D in methanol at 0.0001 and 0.001 ppb had a S/N of 13/1 and 90/1, respectively.

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MarvelX UHPLC Columns

Due to customer demand, IDEX have increased the number of length and ID configurations from our initial eight, to a selection of 55 robust configurations.

MarvelX UHPLC Connection Systems have been designed for easier routing throughout your instrument, with consistent performance and superior re-usability. Built with a convenient, removable stainless steel fitting and changeable precision-cut flexible tubing, MarvelX can be used up to 200 times!

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Public health: how Shimadzu is making a difference

Antibiotics present in food pose a serious public health issue. Allergies to sulfonamides are very common, and the increasing popularity of antibiotics is driving microbial resistance against current antibiotics.

Monitoring the Maximum Residue Levels (MRLs) has proven essential for public health, with the MRLs for some compounds set to low ppb levels. HPLC-MS/MS is very effective at analyzing trace-level antibiotics because it is selective, fast, and very sensitive for all the compounds of interest.

Mandel offers a wide range of Shimadzu LC equpiment. You can get a look at them here.

Read Shimadzu’s application note.